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DIY Stompboxes => Building your own stompbox => Topic started by: Pushtone on March 21, 2006, 02:47:34 AM

Title: Microwave to heat ferric chloride???
Post by: Pushtone on March 21, 2006, 02:47:34 AM

I have an old microwave oven in the garage. Still works.  :icon_idea:

Would it be unsafe to heat up ferric chloride in a microwave before etching?  :icon_eek:

Doesn't need to get boiling hot, just warm.  :icon_confused:

30 seconds ought to do it eh?  :icon_biggrin:
Title: Re: Microwave to heat ferric chloride???
Post by: choklitlove on March 21, 2006, 02:57:27 AM
try it and let us know.



don't die.
Title: Re: Microwave to heat ferric chloride???
Post by: Pushtone on March 21, 2006, 03:00:30 AM
I'm guilty of posting before searching.

Found answer here if your still interested.  :icon_rolleyes:

http://www.diystompboxes.com/smfforum/index.php?topic=27682.0 (http://www.diystompboxes.com/smfforum/index.php?topic=27682.0)

An excellent thread started by Paul Marossy on etching techniques.
Title: Re: Microwave to heat ferric chloride???
Post by: choklitlove on March 21, 2006, 03:03:50 AM
cool, you're still alive and so am i!
Title: Re: Microwave to heat ferric chloride???
Post by: Connoisseur of Distortion on March 21, 2006, 04:25:19 AM
so, it's safe if you never want to use that microwave again? i am a bit lost.
Title: Re: Microwave to heat ferric chloride???
Post by: RaceDriver205 on March 21, 2006, 04:52:44 AM
Quote from: choklitlove on March 21, 2006, 02:57:27 AM
try it and let us know.



don't die.

LOL!  :icon_lol:
Title: Re: Microwave to heat ferric chloride???
Post by: TELEFUNKON on March 21, 2006, 05:45:18 AM
?
I don`t have a microwave oven, and have never used one.
Absolutely no clue, whatsoever.

Wondering however, if a MW could be used to preheat a PCB
or an aluminum box for a couple of seconds to get on temperature
for iron-on layout/design purposes (PnP).
?

anyone got experience or knowledge?
Title: Re: Microwave to heat ferric chloride???
Post by: Paul Perry (Frostwave) on March 21, 2006, 06:53:57 AM
I wouldn't heat ferric chloride in a microwave.
Because, I think there is hydrochloric acid formed by hydrolysis in the mix, and maybe some of this will evaporate out & corrode the insides of the microwave. So it will wreck it in short order, I expect.
It's a while since I was near ferric chloride solution.. does it SMELL acid?? if so, I wouldn't heat it in the oven.
Title: Re: Microwave to heat ferric chloride???
Post by: Ge_Whiz on March 21, 2006, 07:01:48 AM
I would not heat either ferric chloride or metal in a microwave oven. Fumes from the ferric chloride will almost certainly corrode the inside of the oven, including, possibly, the microwave seals causing microwave leakage. Hot spots in the liquid (especially if you re-heat old etch) can cause superheating, leading to a faceful if you're unlucky. Obviously, you can't just say "30s is safe" because it depends on the power of the oven and the amount of etchant.

Placing metal in a microwave causes arcing. This will damage a metal surface, and probably rip tracks up (possibly invisibly) on a PCB. It's also a serious abuse of the magnetron.
Title: Re: Microwave to heat ferric chloride???
Post by: Mark Hammer on March 21, 2006, 08:33:51 AM
I will repeat this until I'm blue in the face.  The only etchant that NEEDS to be heated is that within a short distance and immediately in contact with the board itself.  Heating up the entire etchant bath is simply ONE WAY to accomplish that but it is not required.  You can also point a hair dryer or heat gun at the back of a board that's floating on top of the etchant. or use one of those long-neck halogen study lamps with the bulb pointed down at the PCB from a few inches away.  If the board itself is made warm, then the etchant in immediate contact with it will be warm.  Floating the board at the top of the etchant bath (copper side down, obviously) exposes one side of the board so that it may be easily heated across its entire surface.

If you are desparate to have a warm board, then use the iron employed to put the PCB transfer on to warm up the board before putting it in the etchant.

METAL THINGS DO NOT BELONG IN A MICROWAVE!!!
Title: Re: Microwave to heat ferric chloride???
Post by: R.G. on March 21, 2006, 10:08:01 AM
QuoteWould it be unsafe to heat up ferric chloride in a microwave before etching?
Bad idea, for some of the reasons mentioned here.

It's much simpler to use a home improvements store heat lamp in a clamp-on reflector bulb fitting to heat an open tray. Safer too.

I used to warm up my plastic bottles of etchant by standing them in a sink of hot tap water for 10-15 minutes while I readied all the other paraphernalia.
Title: Re: Microwave to heat ferric chloride???
Post by: TELEFUNKON on March 21, 2006, 10:47:04 AM
OK - after first warnings, I googled a bit
and will stay away from microwaves.

Wouldn`t wanna blow the yellow stuff around (in the kitchen?)
with a hairdryer, though.
Title: Re: Microwave to heat ferric chloride???
Post by: Mark Hammer on March 21, 2006, 10:57:42 AM
Well, you are wise to avoid anything that risks spillage or splattering.  Ferric Chloride is the HIV, avian flu, and hepatitis C of chemicals, rolled into one.  Once you get it on clothing, it's there for life, and it spreads to other things.  Stick a t-shirt with a little bit of FeCl stain in the washer and everything soon has a stain.  Seriously.

Having said that, as liquids go, ferric chloride is fairly heavy, and VERY heavy if it is somewhat used (the copper doesn't magically leave town; it gets added to the weight of the fluid).  If your etchant is sitting in a container whose sides come up at least an inch higher than the fluid level, and the hair dryer/heat-gun is anything less than wind-tunnel force, you should have little problem with splatter if the heat source is at least 2-3 inches back from the board.

All in all, the biggest and best reason for using a lamp as a source of heat rather than a hair dryer is the fact that you can turn the lamp on and walk away.  The heat blowing methods require you to stand there like an idiot for 10 minutes holding a hair dryer while your wrist goes numb.  The very same wrist you will need for drilling and soldering later that day.
Title: Re: Microwave to heat ferric chloride???
Post by: toneman on March 21, 2006, 01:03:19 PM
a small note:
AC -powered hair driers & water *DO NOT* go together!!   :icon_eek:
Even if U are running from a GFI outlet.
I *have* used the microwave "heating technique" after the idea was posted on
this forum a year or so ago.....
It *does* work!!!  U *DO* have to be carefull!!   8)
It enabled me to reuse some FeCl that I knew had some life still in it.
Since then, i've been looking for a used microwave at Goodwill.
I just dedicated a large square tupperware container for my "reheater".
U put metal in microwaves to do browning & bacon crisping.
If U put a spoon, for example, in the m-wave, it will give off sparks.
A dish with any metal in/on it (i.e. gold), might spark or will get warmer than a pure plastic dish.
If this is your *first* or actually *2nd* time working with FeCL, i would recommend the hot water bath for reuse.
I was skeptical, at first, about how this would work, but i did it, and it does work.    8)
I definitely do not like the proposed hair drier technique.    :o
Leave the FeCL in a clear glass or plastic container in the sun for a while.
U can feel the sides to tell how hot it is.  Swirl it around as it heats up. 
Use an infrared therm to do noncontact measurement.
U can only do this in the summer as winter time air defeats your intentions.
Always!!  play it safe---gloves--latex or nitrile, & saftey glasses & work outdoors.
guess that was a big, small note   :D

Title: Re: Microwave to heat ferric chloride???
Post by: Ponchus on March 21, 2006, 04:27:56 PM
I simply put ferric chloride into a plastic container and throw the PCB into it. Then, I fill up a separate (slightly larger) plastic container with boiling water (or very hot tap water) and float the container with the etchant on the boiling water. Lately, I've taken to putting a weight on top of the etchant container, so that it gets pushed into the hot water, rather than just floating on it. Every so often, I replace the hot water. Seems to work fine for me...
Title: Re: Microwave to heat ferric chloride???
Post by: Pushtone on March 21, 2006, 05:58:26 PM
Thanks for all the advice and words of wisdom.

But I think I've found a better way. I have an old electric teapot. Its heating element is designed to be immersed. It could boil the solution but I have a meat thermometer to prevent that. Maybe I can mod it to only get hot and not boil.

Anyway I need a way to heat the ferric chloride because I have to etch far away from AC or a sink. And this is all about etching artwork into Hammond boxes. My tests indicate to me that a hot solution produces cleaner lines. Still testing.
Title: Re: Microwave to heat ferric chloride???
Post by: Peter Snowberg on March 21, 2006, 06:13:38 PM
Quote from: Pushtone on March 21, 2006, 05:58:26 PM
But I think I've found a better way. I have an old electric teapot. Its heating element is designed to be immersed. It could boil the solution but I have a meat thermometer to prevent that. Maybe I can mod it to only get hot and not boil.

:icon_eek:

The ferric chloride will etch away tthe element casing and then you'll have AC energized etchant and an electrical hazard.

They're desiged to be immersed in water not ETCHANT!
Title: Re: Microwave to heat ferric chloride???
Post by: brad on March 21, 2006, 06:18:55 PM
Yikes dude.  Don't worry so much about heating your etch solution.  Just placing the containter in a larger one with a bit of warm water in the bottom of it will do the trick.
Title: Re: Microwave to heat ferric chloride???
Post by: Pushtone on March 21, 2006, 06:39:09 PM
Oops, Right, FeCL eats metal...

Back to the microwave.

Please try to understand brad. This is a totally different type of etching than doing a PCB. I've had to re-learn techniques.
Really hot etchant applied with a paint brush, washed off and reapplied several times makes nice fine lines in the aluminum.

The results speak for themselves.
(http://www3.telus.net/david65/pedal-pics/BSIAB-F34.jpg)

Quote from: Peter Snowberg on March 21, 2006, 06:13:38 PM
Quote from: Pushtone on March 21, 2006, 05:58:26 PM
But I think I've found a better way. I have an old electric teapot. Its heating element is designed to be immersed. It could boil the solution but I have a meat thermometer to prevent that. Maybe I can mod it to only get hot and not boil.

:icon_eek:

The ferric chloride will etch away the element casing and then you'll have AC energized etchant and an electrical hazard.

They're desiged to be immersed in water not ETCHANT!
Title: Re: Microwave to heat ferric chloride???
Post by: sta63bmx on March 21, 2006, 08:30:29 PM
That box is just excellent.  After it was applied, did you let it sit and etch for a little bit and then wipe it off, and repeat?  How long in between "coats"?
Title: Re: Microwave to heat ferric chloride???
Post by: $uperpuma on March 21, 2006, 09:49:26 PM
seems kind of unecessary... I have etched quite a few boards in 15-20 minutes by just warming the solution in hot tap water... seems a little overboard to try to get it to 200 degrees
Title: Re: Microwave to heat ferric chloride???
Post by: brad on March 21, 2006, 10:44:19 PM
Quote from: Pushtone on March 21, 2006, 06:39:09 PM
Please try to understand brad. This is a totally different type of etching than doing a PCB. I've had to re-learn techniques.
Really hot etchant applied with a paint brush, washed off and reapplied several times makes nice fine lines in the aluminum.

The results speak for themselves.
(http://www3.telus.net/david65/pedal-pics/BSIAB-F34.jpg)

Wow!  Great box :D  I didn't realise that's what you were etching.
Title: Re: Microwave to heat ferric chloride???
Post by: bond on March 22, 2006, 12:10:52 AM
that looks just incredible mate
Title: Re: Microwave to heat ferric chloride???
Post by: Pushtone on March 22, 2006, 04:44:16 PM
Thanks,

Member soggybag had some great results to for those interested in etched artwork.
Check out his last thread on the topic.
http://www.diystompboxes.com/smfforum/index.php?topic=35114.0